[ ] SIENA

Stimulation Initiative for European Neural Applications

Esprit Project 9811



Case Studies of Successful Applications



On-line Quality Modelling in Polymer Production

Company background

REPSOL QUÍMICA is the wholly owned subsidiary of Repsol S.A., the most important oil company in Spain and among the first one hundred in the world. REPSOL QUÍMICA is the main Spanish manufacturer of petrochemical products holding a prominent position in the home industrial market. In order to maintain and inhance its competitiveness has as priority technological development programmes in which the current project has been carried out.

Description of the problem

The quality of a polymer made in a REPSOL plant is determined using two independent test: the Melt Index (MI) and the density (DE). The MI is a measure of the flow rate of extrusion of the material through a die while the DE is a measure of the packing of the molecules within the polymer crystals. Both qualities measure the properties of the polymer and they are of great importance when characterising the polymer for practical applications. However, these measurements are costly as well as technically delicate and therefore they are carried out off-line in the laboratory each 2 and 4 hours respectively. Hence, during this period of time no quality measurement of the final product is performed. This is why a model that estimates on-line the value of these properties as a function of the state of the plant would be useful for controlling the final characteristics of polymer. The state of the plant is defined by the set of all variables in the reactor. However, within the great number of variables that determine this state, four of them were identify as those which are mainly responsible of the changes in both the MI and DE values.

Neural Network Application

Neural networks have been proved to be extremely successful in system modelling. However, in industrial environments there often exists an important drawback that is the presence of time varying conditions. Modelling of non-linear system under these conditions leads to the absence of global models and therefore oblige to built adaptive systems using local models. Local models define functions that are applicable only in the neighbourhood of the current state of the plant and they are built using only those states of the plant that were closed to the current one. Two neural network local models were built to estimate the MI and DE values as a function of the four variables that define the state of the plant. The models are updated each time that a new measurement of MI and DE performed in the laboratory was carried out. Meanwhile estimations of MI and DE are obtained using the neural network models.

Benefits

These neural network models offer the possibility of estimating, on-line during its production, the polymer DE and MI values. Therefore, the state of the plant can be changed in order to improve the polymer quality maintaining the MI and DE values within a fixed range of variation.

Generalisation

The system modelling described here is a typical application of modelling in industrial environments where there exists a set of independent variables along with one or two dependent variables. Within industrial environments, it is often found variables that are difficult to measure or there is no simple form of being obtained, therefore a model is required for their estimation.

Contact persons

Guzmán García - Repsol Química - El Morell, Apdo 398 - 43080 Tarragona - Barcelona - Spain.

Alberto Pérez, Instituto de Ingenierí a del Conocimiento - IIC Unversidad Autónoma de Madrid - Módulo C-XVI planta 2 - 28049 Madrid - Spain - Phone: +34 1 397 39 73; Fax: +34 1 397 39 72; E-mail:= alberto@irene.iic.uam.es.